MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\BIZ\\BIZ2016-D07-WJ3.D Tgt Mass (EZX): 409.00 Injection Date : 7 Dec 16 3:32 pm +0800 Seq. Line : 0 Sample Name : BIZ2016-D07-WJ3 Location : P2-B-01 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-100220 Batch#22770 Easy-Access Method: '1-POS-3MIN' 409.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU20001.112100000.5*DAD1 C, Sig=254,4 Ref=off mAU6004001.3001.3471.39520000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701500001000005000000.511.5 Ion 410, MSD1 410,Target Mass 409 +H Positive, EIC=409.7:410.7 10000075000500002500000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min1.24122.5min1.2401.61211.2471.2471.32011..3379451.4331.7481.522.5min*1.522.5min* RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.11 0.03 1.63 1.05 0.08 317 1.25 0.01 1962.73 2652.10 99.31 410 1.32 0.02 5.34 4.84 0.27 410 1.37 0.02 1.48 1.58 0.08 317 1.40 0.02 1.22 1.20 0.06 317 1.43 0.02 2.17 0.45 0.11 317 1.75 0.02 1.83 2.01 0.09 317 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.25 0.01 580.00 828.02 98.08 410 1.30 0.02 4.82 1.65 0.81 410 1.35 0.02 2.70 2.62 0.46 317 1.40 0.03 2.00 1.23 0.34 317 1.61 0.03 1.84 0.57 0.31 317HY-LCMS-02 12/7/2016 16:05:30 KFF(LCMS-02)Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.24 <<<< POSITIVE SPECTRA >>>> ES-API Positive300002500020000 411.315000 317.31000050000200300400500600700800900m/z 410.2HY-LCMS-02 12/7/2016 16:05:30 KFF(LCMS-02)Page
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